Mössbauer Spectrometer MsAa-3 - Mössbauer Spectroscopy Division

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Transcript Mössbauer Spectrometer MsAa-3 - Mössbauer Spectroscopy Division

Mössbauer Spectrometer MsAa-3
Robert Górnicki
RENON
PL-30-732 Kraków, ul. Gliniana 15/15, POLAND
Telephone: +(48-12) 650-6020; Fax: +(48-12) 650-6021
www.renon.strefa.pl [email protected]
Artur Błachowski and Krzysztof Ruebenbauer
Mössbauer Spectroscopy Division, Institute of Physics
Pedagogical University
PL-30-084 Kraków, ul. Podchorążych 2, POLAND
Telephone: +(48-12) 662-6317, 19; Fax: +(48-12) 637-2243
www.elektron.ap.krakow.pl [email protected]
General layout - schematic
More realistic diagram
Spectrometer and SOFTWARE on the NETWORK
General properties
Two types of standard detector heads (proportional and scintillation detector) with the integrated pre-amplifier and high voltage power
supply remotely controlled via the computer.
Additional signal input from typical custom pre-amplifiers and additional input from the external single channel analyzers.
Four spectra collected simultaneously: two Mössbauer spectra and a γ-ray spectrum (collected simultaneously in the coincidence and
anti-coincidence mode with the single channel analyzer window). One of the Mössbauer spectra could be replaced by the laser
velocity calibration data. All four spectra are collected in 4096 channels having 32-bit capacity each.
Robust and high precision transducer with non-linearity well below 0.1 %. It is equipped with the central clear bore tube, and a system
to set up and maintain desired average position of the source. It could be operated either vertically or horizontally.
Down-loadable velocity reference function generated by means of the software in 8192 points. Velocity digital to analog converter has
12-bit precision and it could be operated in the wide range of the repetition frequency (from a fraction till 60 Hz).
High precision laser velocity calibration unit, having very low sensitivity to the external vibrations. The transducer clear bore allows for
a laser beam to be delivered to the moving corner-prism mounted directly behind the source.
Low voltage power supply, buffered by the high capacity rechargeable maintenance free battery allowing for several hours of
uninterrupted operation since the power failure.
All settings (except manual tuning of the PZC circuit for the detector head) are available from the software panel of the controlling
computer. They could be stored on the computer disk and reloaded assuring stable conditions of operation.
Communication with the external world is performed via the Ethernet-Tx TCP/IP link. Hence, the spectrometer could be set as the
stand-alone entity in the Internet.
Versatile thermometric unit with the simple temperature controller being able to control basic functions of the spectrometer.
Data evaluation software Mosgraf allowing to process almost any Mössbauer spectrum of any resonant transition.
-ray spectrometer
Various reference functions
(a) constant velocity
(b) linear velocity
Transducer performance
More performance data
More details on the velocity
error
Error correction based on the
oscilloscope data
Time averaged data
(128 or 512 cycles)
Laser calibration system
RAW SIGNAL
Laser calibration
Laser velocity calibration - errors
Multi-scaler functions
Mosgraf laser calibration