Transcript Regulation_152_2008_plain

COMMISSION REGULATION (EC) No 152/2009
of 27 January 2009
laying down the methods of sampling and analysis for
the official control of feed
Ing. Petrová Jaroslava
Workshop on Official Controls of Feed AGR 46230, 6. – 7. 12. 2011, Ankara. Turkey
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Content of
„Methods of analysis for the official control of feed „
presentation
1. Legal reasons for analysis food samples for the
official control Identification of methods
2. Laboratory requirements
3. History of Methods of analysis for the official
control of feed
4. Content of Regulation 152/2009
5. Analytical methods other than methods for official
control
6. Requirements on methods validated in one
laboratory
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Regulation 767/2009 - Official control in laboratory
(in the placing on the market and use of feed,)
ANNEX I
- Chemical impurities from techological process,
- botanical impuritues
Annex V, VI
- iron level in milk replacers
- Crude protein
- denaturants, binders
- Crude fibre
- ash insoluble in HCl
- Starch
- water content
- crude fat and oil
-crude ash
Article 15
- lysin, methionin
- addives
- Ca, Na, P, Mg
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Regulation 882/2004
on official controls performed to ensure the verification of
compliance with feed and food law, animal health and animal
welfare rules
Article 12
- Laboratory(ies) for official
control are named by
competend national authorities
- Laboratory(ies) for official
control should be accredited
(EN ISO/IEC 17025 on ‘General
requirements for the
competence of testing and
calibration laboratories)
(ÚKZÚZ is accredited since 1994)
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Summary
- Official control obey the same legislation as
production
- Analytical laboratories should be accredited
and analytical method should be validated
- Official analytical method ensure credibility
and comparability of laboratory results
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Methods of analysis for the official control of feed - History
1970 – Directive 70/373/EEC
Directives establishing Community methods of analysis for
the official control of feedingstuffs:
1971 – First Commission Directive 71/250/EEC of 15 June 1971.
Second Commission Directive 71/393/EEC of 18 November 1971
Third Commission Directive 72/199/EEC of 27 April 1971
1972 - Fourth Commission Directive 73/46/EEC of 5 December 1972
1976 - Seventh Commission Directive 76/372/EEC of 1 March 1976
1978- Eight Commission Directive 78/633/EEC of 15 June 1978
1981 - Ninth Commission Directive 81/715/EEC of 31 July 1981
1984 - Tenth Commission Directive 84/425/EEC of 25 July 1984
1993 - Eleventh Commission Directive 93/70/EEC of 28 July 1993 2003 Commission Directive 2003/126/EC of 23 December 2003 on the
analytical method for the determination of constituents of animal
origin for the official control of feedingstuffs
….2009
2009- COMMISSION REGULATION
(EC) No 152/2009 of 27 January
2009 laying down the methods
of sampling and analysis for the
official control of feed
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Regulation 152/2009 methods of analysis
ANNEX II GENERAL PROVISIONS ON METHODS OF
ANALYSIS FOR FEED
C. APPLICATION OF METHODS OF ANALYSIS AND EXPRESSION OF
THE RESULTS
1. Extraction procedure
Several methods determine a specific extraction procedure. As a general
rule, other extraction procedures than the procedure referred to in the
method can be applied on the condition that the used extraction procedure
has been proven to have the equivalent extraction efficiency for the matrix
analysed as the procedure mentioned in the method
2. Clean-up procedure
Several methods determine a specific clean-up procedure. As a general
rule, other clean-up procedures than the procedure referred to in the
method can be applied on the condition that the used clean-up procedure
has been proven to result in equivalent analytical results for the matrix
analysed as the procedure mentioned in the method
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Regulation 152/2009 methods of analysis
Annex III – Methods of Analysis to Control the Composition of Feed
Materials and Compound Feed
A. Determination of moisture
B. Determination of moisture in animal and vegetable fats and oils
C. Determination of the content of crude protein
D. Determination of urea
E. Determination of volatile nitrogenous bases
F. Determination of amino acids (except tryptophane)
G. Determination of tryptophane
H. Determination of crude oils and fats
I. Determination of crude fibre
J. Determination of sugar
K. Determination of lactose
L. Determination of starch – polarimetric method
M. Determination of crude ash
N. Determination of ash which is insoluble in hydrochloric acid
O. Determination of carbonates
P. Determination of total phosphorus – photometric method
Q. Determination of chlorine from chlorides
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Regulation 152/2009 methods of analysis
Annex IV - Methods of Analysis to Control the Level of Authorised Additives
in Feed
A. Determination of vitamin A
B. Determination of vitamin E
C. Determination of the trace elements iron, copper, manganese and zinc
D. Determination of halofuginone
E. Determination of robenidine
F. Determination of diclazuril
G. Determination of lasalocid sodium
Annex V - METHODS OF ANALYSIS TO CONTROL
UNDESIRABLE SUBSTANCES IN FEED
A. Determination of free and total gossypol
B. Determination of the level of dioxins (PCDD/PCDF) and
dioxin-like PCBs
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Regulation 152/2009 methods of analysis
Annex VI - Methods of analysis for the determination
of constituents of animal origin for the official control of
feed - Conditions for the microscopic detection,
identification or estimation of constituents of animal
origin in feed
Annex VIII - methods of analysis to control illegal presence of no longer
authorised additives in feed vi - methods of analysis for the determination
of constituents of animal origin for the official control of feed
Important notes:
More sensitive methods of analysis than the methods of analysis mentioned in this Annex can be used to
detect the illegal presence of no longer authorised additives in feed. The methods of analysis mentioned in
this Annex shall be used for confirmatory purposes.
A. Determination of methyl benzoquate
B. Determination of olachindox
C. Determination of amprolium
D. Determination of carbadox
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Regulation 882/2004 - Methods of sampling and analysis
Article 11
Sampling and analysis methods used in the context of official
controls shall comply with relevant Community rules (152/2009)
or,
(a) if no such rules exist, with internationally recognised rules or
protocols, for example those that the European Committee for
Standardisation (CEN) has accepted or those agreed in national
legislation;
or,
(b) in the absence of the above, with other methods fit for the
intended purpose or developed in accordance with scientific
protocols
Where paragraph 1 does not apply,
validation of methods of analysis may take
place within a single laboratory according
to an internationally accepted protocol.
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CHARACTERISATION OF METHODS OF ANALYSIS
Regulation 882/2004 – Annex III
Wherever possible, methods of analysis shall be characterised by the
appropriate criteria set:
(a) accuracy;
(b) applicability (matrix and concentration range);
(c) limit of detection;
(d) limit of determination;
(e) precision;
(f) repeatability;
(g) reproducibility;
(h) recovery;
(i) selectivity;
(j) sensitivity;
(k) linearity;
(l) measurement uncertainty;
(m) other criteria that may be selected as required.
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Thanks for your attention
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